vialroom

#test-results 2026-06-29

Monday46 messages9 participantstimes are UTC
Highlights from this day
  • VialBot — Verification log updated: WXT — evidence added, status unchanged. 16:45
  • ms_ms_mira — my result contradicts the supplier certificate, do i tell them 16:46
  • deamidation — post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later 17:28
  • deamidation — my sheet has 3 lots from JEEP with a spread under a point, which is tight 18:52
HH

a supplier disputing a result is rare here and it has never gone well for the supplier

log the boring results too. a channel that only records failures produces a false picture, ymmv

HH

whats the underfill rate people are actually seeing

coming back after 11 months with a follow up result, where do i put it

MM

weigh the vial before you reconstitute. it costs nothing and catches the common failure

SD

assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem

VB

Verification log updated: WXT — evidence added, status unchanged.

SD

the honest limits: hobby chain of custody is weak and any result here should be read with that in mind

SD

unrelated but how much does sample handling on my end affect the number

📉5
PS

i have never regretted spending the money on a test. i have regretted not testing twice

🤝5

do the results in this channel skew because people test when suspicious

DE

post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later

💀4🎉5🧊3

one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally

slightly off topic but 99.2 against a certificate of 99 is fine. the same supplier landing low four times in a row is a question, happy to be corrected

underfill is more common than impurity. if you only test purity you are testing the less likely failure

thats a fill problem

EvidenceCounts?
Independent report, lot you bought, lot number legibleyes
Independent report, no lot numberno
Supplier certificate onlyno
Screenshot of a reportno
Blinded pooled submissionyes, for the pool
A friend who said it was fineno

thats within range

PS

the results in this channel skew because people test when they are suspicious. that is selection bias and it is real, for what its worth

🎉2📈4
PS

the widest spread in my data is about 2.6 percentage points across five lots from one supplier

for the archive my vial assayed under label but the purity was fine, which matters more

one data point

PS

sample handling on your end absolutely affects it. draw cleanly, ship fast, do not let it sit warm

VB

Channel stats, last 30 days: 41 messages from 48 members.

DE

my sheet has 3 lots from JEEP with a spread under a point, which is tight

🧊1💀2🤝1

how many lots do you need before you can say anything about a supplier

DE

follow up i had a result i am fairly sure was a handling error on my side and i logged it as such

quantity testing is usually a separate line item and it is the one worth paying for

attach the pdf

⚠️2🧪1
VO

unrelated but i test roughly every tenth vial. it is a sampling strategy, not paranoia

i told KP about a result they would not have liked and they did not argue. credit where it is due

MM

a single sample tells you about a single vial. that is genuinely all it tells you