test it again
#test-results 2026-01-13
- cat_on_the_tray — underfill is more common than impurity. if you only test purity you are testing the less likely failure if the vial has been through a bad transit you are testing the… 16:41
- ari_arrives — weigh the vial before you reconstitute. it costs nothing and catches the common failure 17:04
- first_month_fi — a point or two between the certificate and an independent result is inside what two labs disagree by 17:32
- first_month_fi — my sheet has 8 lots from QSC with a spread under a point, which is tight 17:44
- VialBot — Verification log updated: WWB — evidence added, status unchanged. 17:51
assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem
underfill is more common than impurity. if you only test purity you are testing the less likely failure
if the vial has been through a bad transit you are testing the transit as much as the supplier
one data point
a supplier disputing a result is rare here and it has never gone well for the supplier
attach the pdf
is it worth testing if the vial has already been through a warm transit
post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later
weigh the vial before you reconstitute. it costs nothing and catches the common failure
whats the underfill rate people are actually seeing
a supplier disputing a result is rare here and it has never gone well for the supplier
a point or two between the certificate and an independent result is inside what two labs disagree by
my sheet has 8 lots from QSC with a spread under a point, which is tight
if you are testing to settle an argument you will not settle it with n of 1
[edited]Verification log updated: WWB — evidence added, status unchanged.
what interests me is when the gap goes the same direction every time. once is noise, three times is a pattern
log the boring ones
while im here the results in this channel skew because people test when they are suspicious. that is selection bias and it is real
weigh it first
| Evidence | Counts? |
|---|---|
| Independent report, lot you bought, lot number legible | yes |
| Independent report, no lot number | no |
| Supplier certificate only | no |
| Screenshot of a report | no |
| Blinded pooled submission | yes, for the pool |
| A friend who said it was fine | no |
nice result