vialroom

#test-results 2024-07-08

Monday35 messages6 participantstimes are UTC
Highlights from this day
  • area_percent — the results in this channel skew because people test when they are suspicious. that is selection bias and it is real 22:10
  • third_shift — quantity testing is usually a separate line item and it is the one worth paying for, thats just me 22:21
  • luerlok — a single sample tells you about a single vial. that is genuinely all it tells you i had a result i am fairly sure was a handling error on my side and i logged it as… 23:01
  • logrotate — log the boring results too. a channel that only records failures produces a false picture 23:03
  • logrotate — one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally 23:14

i test roughly every tenth vial. it is a sampling strategy, not paranoia, i have it written down somewhere

nice result

TE

weigh it first

peptidemeter-summary-a-2601.pdf
2 pages · 260 KB · not retained in the public archive
22:00tenpence pinned a message
TE

a supplier disputing a result is rare here and it has never gone well for the supplier

the results in this channel skew because people test when they are suspicious. that is selection bias and it is real

the widest spread in my data is about 2.6 percentage points across five lots from one supplier

*VendorInvestigate not the other one

the honest limits: hobby chain of custody is weak and any result here should be read with that in mind

quantity testing is usually a separate line item and it is the one worth paying for, thats just me

16

log the boring ones

whats the lot

selection bias

LU

for the archive does anyone log the negative results, the boring ones

unrelated but how do you separate batch variance from supplier variance

test it again

LO

update from 7 months ago: retested the same supplier, result came back better, logged both, your mileage will differ

i had a result i am fairly sure was a handling error on my side and i logged it as such

LU

post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later

LO

99 against a certificate of 97.4 is fine. the same supplier landing low four times in a row is a question

underfill is more common than impurity. if you only test purity you are testing the less likely failure

LU

sample handling on your end absolutely affects it. draw cleanly, ship fast, do not let it sit warm

weigh the vial before you reconstitute. it costs nothing and catches the common failure

a single sample tells you about a single vial. that is genuinely all it tells you
i had a result i am fairly sure was a handling error on my side and i logged it as such

LO

log the boring results too. a channel that only records failures produces a false picture

😂96
LO

one bad test does not condemn a supplier. one good test does not clear one. both halves get ignored equally

👍1😂1🤝1

log the lot number

a single sample tells you about a single vial. that is genuinely all it tells you

a result without a lot number and a purchase date is an anecdote with a pdf attached, ymmv