vialroom

#test-results 2024-07-03

Wednesday22 messages7 participantstimes are UTC
Highlights from this day
  • u100_pat — whats the underfill rate people are actually seeing the results in this channel skew because people test when they are suspicious. that is selection bias and it is real 12:48
  • deadspace — while im here i had a result i am fairly sure was a handling error on my side and i logged it as such assay under label with good purity means you got less of the… 13:28
  • VialBot — Archive lookup: HPLC_Hank first appears in this channel on 2024-02-09. 14:24
  • HPLC_Hank — weigh the vial before you reconstitute. it costs nothing and catches the common failure 17:47
  • deadspace — my sheet has 8 lots from BCH with a spread under a point, which is tight 17:48
U1

whats the underfill rate people are actually seeing
the results in this channel skew because people test when they are suspicious. that is selection bias and it is real

post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later

HH

while im here does a bad result on one lot condemn the whole supplier

DE

while im here i had a result i am fairly sure was a handling error on my side and i logged it as such
assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem

peptidemeter-summary-b-0114.pdf
2 pages · 510 KB · not retained in the public archive
VB

Archive lookup: HPLC_Hank first appears in this channel on 2024-02-09.

U1

do the results in this channel skew because people test when suspicious

HH

99.4 against a certificate of 96.8 is fine. the same supplier landing low four times in a row is a question

HH

the widest spread in my data is about 2.6 percentage points across five lots from one supplier

VV

posting my VendorInvestigate result on lot D-0718, what do people make of it

VV

follow up a point or two between the certificate and an independent result is inside what two labs disagree by, n of 1 obviously

VV

i test roughly every tenth vial. it is a sampling strategy, not paranoia

how much does sample handling on my end affect the number

HH

my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ, someone check my working

HH

weigh the vial before you reconstitute. it costs nothing and catches the common failure

🧊17👀1
DE

my sheet has 8 lots from BCH with a spread under a point, which is tight

PS

update on the earlier thing whats the worst result anyone has logged and what happened next