whats the underfill rate people are actually seeing
the results in this channel skew because people test when they are suspicious. that is selection bias and it is real
#test-results 2024-07-03
- u100_pat — whats the underfill rate people are actually seeing the results in this channel skew because people test when they are suspicious. that is selection bias and it is real 12:48
- deadspace — while im here i had a result i am fairly sure was a handling error on my side and i logged it as such assay under label with good purity means you got less of the… 13:28
- VialBot — Archive lookup: HPLC_Hank first appears in this channel on 2024-02-09. 14:24
- HPLC_Hank — weigh the vial before you reconstitute. it costs nothing and catches the common failure 17:47
- deadspace — my sheet has 8 lots from BCH with a spread under a point, which is tight 17:48
post the lot, the purchase month, the lab, the number, and what you were expecting. that makes it useful later
while im here does a bad result on one lot condemn the whole supplier
while im here i had a result i am fairly sure was a handling error on my side and i logged it as such
assay under label with good purity means you got less of the right thing. that is a fill problem, not a synthesis problem
how do you separate batch variance from supplier variance
selection bias
nice result
Archive lookup: HPLC_Hank first appears in this channel on 2024-02-09.
do the results in this channel skew because people test when suspicious
99.4 against a certificate of 96.8 is fine. the same supplier landing low four times in a row is a question
the widest spread in my data is about 2.6 percentage points across five lots from one supplier
posting my VendorInvestigate result on lot D-0718, what do people make of it
thats a fill problem
follow up a point or two between the certificate and an independent result is inside what two labs disagree by, n of 1 obviously
which lab
i test roughly every tenth vial. it is a sampling strategy, not paranoia
how much does sample handling on my end affect the number
do you test every order or sample it
my read after three years of this: purity is mostly fine across the market and fill consistency is where suppliers differ, someone check my working
weigh the vial before you reconstitute. it costs nothing and catches the common failure
my sheet has 8 lots from BCH with a spread under a point, which is tight
update on the earlier thing whats the worst result anyone has logged and what happened next