i would rather fund one careful quantity test than three purity tests
#lab-requests 2025-07-12
- VialBot — Inter-lab diff for lot D-0718: 98.1% vs 98.6%. Within expected range. 19:50
- LC_MS_Lena — i keep half the sample back so there is something to send if the first one goes missing 19:59
- typosquat_tay — while im here quantity is the test worth paying for. purity is usually fine and fill usually is not, not advice obviously 20:23
- typosquat_tay — including a reference standard in the batch is the single best thing we ever added to this process 20:35
- tail_factor — chain of custody in hobby testing is weak and we say so in every writeup 21:36
what happens if a submission gets lost in transit
we have never had a lab mix up a sample. we have had members mix up their own labelling twice
submissions go out blinded. the lab gets a code, not a supplier name. that removes one variable, it is not distrust
a pooled result tells you about the pool. it does not tell you about your vial
VendorInvestigate has been the fastest for us. PeptideMeter has been the most detailed. those are not the same lab
right so two labs on the same lot is a luxury but it is how we learned what inter-lab variance looks like
Inter-lab diff for lot D-0718: 98.1% vs 98.6%. Within expected range.
i keep half the sample back so there is something to send if the first one goes missing
update from 25 months ago: the blinding process is unchanged and it has held up fine
the split works from about 9 people. below that everyone pays more than the test is worth, still working it out
is there a preferred lab for quantity specifically
label the syringe
add a standard
while im here quantity is the test worth paying for. purity is usually fine and fill usually is not, not advice obviously
code not name
is there a submission going out this month and can i get in on it
are we blinding this one or does the lab know the source
what compound should we prioritise for the next round
including a reference standard in the batch is the single best thing we ever added to this process
blinded obviously
we publish the raw report. summaries hide the thing you needed to see
count me in
is there a queue position i can check
thats the turnaround
dont send your only vial
in for one
a code and a lot number on the syringe in permanent marker. that is the whole labelling requirement
chain of custody in hobby testing is weak and we say so in every writeup
who is coordinating this round
declare it as an analytical reference sample with a low value. that is what it is, still working it out
queue is posted
i coordinate the round, collect the codes, and post every result including the dull ones, anyway
unrelated but send a capped syringe with enough for a rerun. the minimum is never enough if they need to repeat it