vialroom

#coa-reading 2025-11-26

Wednesday15 messages4 participantstimes are UTC
Highlights from this day
  • pioneer_pia — quick one if you only read one line on a certificate, read the lot number. if you read two, read the assay, still working it out 21:43
  • ferritin_fay — the retention time on this one is different from the last lot, problem i asked SGN for the method and they sent it. that alone put them ahead of most 22:12
  • pioneer_pia — the certificate from WWB is the one i use to teach this because it actually has a populated impurity table 22:22
  • tokyo_taper — i keep every certificate in a dated folder and compare them. two suppliers had not changed their template since 2019 22:28
PP

genuine question is area percent the same thing as how many mg are in the vial

purity is what fraction of the contents is the target. assay is how many mg are actually there. different questions

check the lot

PP

quick one if you only read one line on a certificate, read the lot number. if you read two, read the assay, still working it out

FF

the retention time on this one is different from the last lot, problem
i asked SGN for the method and they sent it. that alone put them ahead of most

lot        bought    purity   assay/label
A-2418     2025-03   99.1%    9.6 / 10mg
A-2601     2025-08   98.7%    9.8 / 10mg
B-0114     2026-01   99.3%    9.4 / 10mg
B-0329     2026-04   98.9%    9.9 / 10mg
👍217

the three way match is vial, certificate, invoice. if all three agree you have something

the certificate from WWB is the one i use to teach this because it actually has a populated impurity table

🔥4💀11😂1

the paperwork can be perfect and the vial can still be light. weigh it

i keep every certificate in a dated folder and compare them. two suppliers had not changed their template since 2019

lot-log.csv
511 rows · not retained in the public archive
AA

water content is why an honest 10mg vial assays at 9.1. karl fischer titration, and most certificates omit it